| | EPA RECOMMENDED SW-846 METHODS OF ANALYSIS |
| | 2,34 | | MB |
| | 1200 | | stron |
| | 702 | | ID | UNITED STATES ENVIRONMENTAL PROTECTION AGENCY |
| | 1998 | | rok |
| | EPA RECOMMENDED SW-846 METHODS OF ANALYSIS |
| | VOLUME ONE SECTION A |
| | DISCLAIMER |
| | ABSTRACT |
| | TABLE OF CONTENTS |
| | METHOD INDEX AND CONVERSION TABLE |
| | PREFACE |
| | ACKNOWLEDGEMENTS |
| | PART I METHODS FOR ANALYTES AND PROPERTIES |
| | CHAPTER ONE -- QUALITY CONTROL |
| | 1.0 Introduction |
| | 2.0 QA Project Plan |
| | 3.0 Field Operations |
| | 4.0 Laboratory Operations |
| | 5.0 Definitions |
| | 6.0 References |
| | CHAPTER TWO -- CHOOSING THE CORRECT PROCEDURE |
| | 2.1 Purpose |
| | 2.2 Required Information |
| | 2.3 Implementing the Guidance |
| | 2.4 Characteristics |
| | 2.5 Ground Water |
| | 2.6 References |
| | CHAPTER THREE -- INORGANIC ANALYTES |
| | 3.1 Sampling Considerations |
| | 3.2 Sample Preparation Methods |
| | Method 3005A: Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analysis by |
| | FLAA or ICP Spectroscopy |
| | Method 3010A: Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by |
| | FLAA or ICP Spectroscopy |
| | Method 3015: Microwave Assisted Acid Digestion of Aqueous Samples and Extracts |
| | Method 3020A: Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by |
| | GFAA Spectroscopy |
| | Method 3031: Acid Digestion of Oils for Metals Analysis by Atomic Absorption or ICP Spectrometry |
| | |
| | Method 3040A: Dissolution Procedure for Oils, Greases, or Waxes |
| | Method 3050B: Acid Digestion of Sediments, Sludges, and Soils |
| | Method 3051: Microwave Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils |
| | Method 3052: Microwave Assisted Acid Digestion of Siliceous and Organically Based Matrices |
| | Method 3060A: Alkaline Digestion for Hexavalent Chromium |
| | 3.3 Methods for Determination of Inorganic Analytes |
| | Method 6010B: Inductively Coupled Plasma-Atomic Emission Spectrometry |
| | Method 6020: Inductively Coupled Plasma-Mass Spectrometry |
| | Method 7000A: Atomic Absorption Methods |
| | Method 7020: Aluminum (Atomic Absorption, Direct Aspiration) |
| | Method 7040: Antimony (Atomic Absorption, Direct Aspiration) |
| | Method 7041: Antimony (Atomic Absorption, Furnace Technique) |
| | Method 7060A: Arsenic (Atomic Absorption, Furnace Technique) |
| | Method 7061A: Arsenic (Atomic Absorption, Gaseous Hydride) |
| | Method 7062: Antimony and Arsenic (Atomic Absorption, Borohydride Reduction) |
| | Method 7063: Arsenic in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) |
| | Method 7080A: Barium (Atomic Absorption, Direct Aspiration) |
| | Method 7081: Barium (Atomic Absorption, Furnace Technique) |
| | Method 7090: Beryllium (Atomic Absorption, Direct Aspiration) |
| | Method 7091: Beryllium (Atomic Absorption, Furnace Technique) |
| | Method 7130: Cadmium (Atomic Absorption, Direct Aspiration) |
| | Method 7131A: Cadmium (Atomic Absorption, Furnace Technique) |
| | Method 7140: Calcium (Atomic Absorption, Direct Aspiration) |
| | Method 7190: Chromium (Atomic Absorption, Direct Aspiration) |
| | Method 7191: Chromium (Atomic Absorption, Furnace Technique) |
| | Method 7195: Chromium, Hexavalent (Coprecipitation) |
| | Method 7196A: Chromium, Hexavalent (Colorimetric) |
| | Method 7197: Chromium, Hexavalent (Chelation/Extraction) |
| | Method 7198: Chromium, Hexavalent (Differential Pulse Polarography) |
| | Method 7199: Determination of Hexavalent Chromium in Drinking Water, Groundwater and Industrial |
| | Wastewater Effluents by Ion Chromatography |
| | Method 7200: Cobalt (Atomic Absorption, Direct Aspiration) |
| | Method 7201: Cobalt (Atomic Absorption, Furnace Technique) |
| | Method 7210: Copper (Atomic Absorption, Direct Aspiration) |
| | Method 7211: Copper (Atomic Absorption, Furnace Technique) |
| | Method 7380: Iron (Atomic Absorption, Direct Aspiration) |
| | Method 7381: Iron (Atomic Absorption, Furnace Technique) |
| | Method 7420: Lead (Atomic Absorption, Direct Aspiration) |
| | Method 7421: Lead (Atomic Absorption, Furnace Technique) |
| | Method 7430: Lithium (Atomic Absorption, Direct Aspiration) |
| | Method 7450: Magnesium (Atomic Absorption, Direct Aspiration) |
| | Method 7460: Manganese (Atomic Absorption, Direct Aspiration) |
| | Method 7461: Manganese (Atomic Absorption, Furnace Technique) |
| | Method 7470A: Mercury in Liquid Waste (Manual Cold-Vapor Technique) |
| | Method 7471A: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique) |
| | Method 7472: Mercury in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) |
| | Method 7480: Molybdenum (Atomic Absorption, Direct Aspiration) |
| | Method 7481: Molybdenum (Atomic Absorption, Furnace Technique) |
| | Method 7520: Nickel (Atomic Absorption, Direct Aspiration) |
| | Method 7521: Nickel (Atomic Absorption, Furnace Method) |
| | Method 7550: Osmium (Atomic Absorption, Direct Aspiration) |
| | Method 7580: White Phosphorus (P ) by Solvent Extraction and Gas 4 Chromatography |
| | Method 7610: Potassium (Atomic Absorption, Direct Aspiration) |
| | Method 7740: Selenium (Atomic Absorption, Furnace Technique) |
| | Method 7741A: Selenium (Atomic Absorption, Gaseous Hydride) |
| | Method 7742: Selenium (Atomic Absorption, Borohydride Reduction) |
| | Method 7760A: Silver (Atomic Absorption, Direct Aspiration) |
| | Method 7761: Silver (Atomic Absorption, Furnace Technique) |
| | Method 7770: Sodium (Atomic Absorption, Direct Aspiration) |
| | Method 7780: Strontium (Atomic Absorption, Direct Aspiration) |
| | Method 7840: Thallium (Atomic Absorption, Direct Aspiration) |
| | Method 7841: Thallium (Atomic Absorption, Furnace Technique) |
| | Method 7870: Tin (Atomic Absorption, Direct Aspiration) |
| | Method 7910: Vanadium (Atomic Absorption, Direct Aspiration) |
| | Method 7911: Vanadium (Atomic Absorption, Furnace Technique) |
| | Method 7950: Zinc (Atomic Absorption, Direct Aspiration) |
| | Method 7951: Zinc (Atomic Absorption, Furnace Technique) |
| | APPENDIX -- COMPANY REFERENCES |
| | VOLUME ONE SECTION B |
| | CHAPTER FOUR -- ORGANIC ANALYTES |
| | 4.1 Sampling Considerations |
| | 4.2 Sample Preparation Methods |
| | 4.2.1 Extractions and Preparations |
| | Method 3500B: Organic Extraction and Sample Preparation |
| | Method 3510C: Separatory Funnel Liquid-Liquid Extraction |
| | Method 3520C: Continuous Liquid-Liquid Extraction |
| | Method 3535: Solid-Phase Extraction (SPE) |
| | Method 3540C: Soxhlet Extraction |
| | Method 3541: Automated Soxhlet Extraction |
| | Method 3542: Extraction of Semivolatile Analytes Collected Using Method 0010 (Modified Method 5 |
| | Sampling Train) |
| | Method 3545: Pressurized Fluid Extraction (PFE) |
| | Method 3550B: Ultrasonic Extraction |
| | Method 3560: Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons |
| | Method 3561: Supercritical Fluid Extraction of Polynuclear Aromatic Hydrocarbons |
| | Method 3580A: Waste Dilution |
| | Method 3585: Waste Dilution for Volatile Organics |
| | Method 5000: Sample Preparation for Volatile Organic Compounds |
| | Method 5021: Volatile Organic Compounds in Soils and Other Solid Matrices Using Equilibrium |
| | Headspace Analysis |
| | Method 5030B: Purge-and-Trap for Aqueous Samples |
| | Method 5031: Volatile, Nonpurgeable, Water-Soluble Compounds by Azeotropic Distillation |
| | Method 5032: Volatile Organic Compounds by Vacuum Distillation |
| | Method 5035: Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste |
| | Samples |
| | Method 5041A: Analysis for Desorption of Sorbent Cartridges from Volatile Organic Sampling Train |
| | (VOST) |
| | 4.2.2 Cleanup |
| | Method 3600C: Cleanup |
| | Method 3610B: Alumina Cleanup |
| | Method 3611B: Alumina Column Cleanup and Separation of Petroleum Wastes |
| | Method 3620B: Florisil Cleanup |
| | Method 3630C: Silica Gel Cleanup |
| | Method 3640A: Gel-Permeation Cleanup |
| | Method 3650B: Acid-Base Partition Cleanup |
| | Method 3660B: Sulfur Cleanup |
| | Method 3665A: Sulfuric Acid/Permanganate Cleanup |
| | 4.3 Determination of Organic Analytes |
| | 4.3.1 Gas Chromatographic Methods |
| | Method 8000B: Determinative Chromatographic Separations |
| | Method 8011: 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by |